Added: Dwain Toomey - Date: 08.09.2021 04:40 - Views: 38199 - Clicks: 5174
Shut Up and Listen! Crushing It! Related Audiobooks Free with a 30 day trial from Scribd. Ladies Get Paid Claire Wasserman. Think Like a Billionaire James Altucher. Gundry, MD. Full Name Comment goes here. Are you sure you want to Yes No.
Ahmad Reza Naseri. Show More. No Downlo. Views Total views. Actions Shares. No notes for slide. Method B: Wash sudaphed tablets in cold water until most it's impossible to get all of it of the red coating is gone. Put the tablets in hot water, heat them to boiling, and stir until the tablets have completely dissolved.
Filter off the liquid. The amount of water the pseudo- ephedrine [I'll call it ephedrine from now on for simplicity] is dissolved in is not too important - it should be as little as possible, but at least as much as the amount of sulfuric acid that is added later to insure to that the potassium dichromate dissolves. To this aqueous mixture add 0. If you used sudaphed tablets, figure by the theoretical amount in solution of tablets X content of each tablet.
Slowly add 3ml Sulfuric for each gram ephedrine, stirring as you add it. Let react for minutes. Basify the solution with concentrated sodium hydroxide solution until you see the solution become a bright green green with a white precipitate - the methcathinone.
This happens above pH 8. Try not to add too much hydroxide if you do the solution becomes black and there is probably some decomposition of the methcathinone. Extract times with naptha add the naptha, shake it up, pour off as much naptha as you can - but DON'T get ANY reaction mixture in the extracts!
Use as much naptha as would equal about percent of the reaction mixture. Shake the mixture, extract off the aqueous lower portion. This is an acid solution of the methcathinone. Add acetone and stir it a little. Continue evaporating and adding acetone until it does. Be careful not to burn the thick mixture adding acetone helps keep the temperature down. Remove from the freezer, filter the crystals off and wash with a small amount of cold 2.
I wouldn't take more than 20mg for a first dose, and I wouldn't take it if I had a history of heart disease or stroke in the family, or if I had high blood pressure. Really, really habit forming. Very, very pleasurable. Don't introduce this stuff to kids or sell it or I will personally hunt you down. Substitutions of potassium hydroxide for sodium hydroxide, sodium dichromate for potassium dichromate and similar subsitution will not have an impact. I wouldn't substitute anything for the sulfuric acid, however. HCl is used to make the drug salt because it is so easy to evaporate the excess off.
Any method of making drug salts you are familiar with should be satisfactory. Ether works a little better than naptha, but it's more dangerous. I stay away from it. It isn't hard, but the posted synthesis cannot lead to good becuase of certain ommisions. I don't know if these were omitted deliberately as to stop non-chemists from completing it or whether the author of the original article just forgot.
In any case, here are some things you should be aware of. This will lead to a very thick reaction mixture. When extracting with naphta this thickness will prevent separation of layers. The naphta will stay in suspension and the naphta that does separate will not contain high amounts of CAT. This le to unacceptably low yields. Use about 10 ml. Do not use tap-water, get de-mineralised water. Trace amounts of minerals will inhibit the reaction. If you don't, local concentrations will get too high, causing the ephedrine to break down. Stir well while adding the H2SO4.
The heat developed during this stage will cause practicaly all the CAT to break down if you don't. The best way to cool it is as follows: Place the reaction mixture 3. This will cause the temperature to drop another couple of degrees, ensuring a good cooling. Again, the high temperature would cause the CAT to disintegrate. The anonymous chemist. Due to the double-blind, any mail replies to this message will be anonymized, and an anonymous id will be allocated automatically. You have been warned. Please report any problems, inappropriate use etc.
Eye protection is needed and this is done in a well-ventilated area. This article is for information purposes only. All of these chemicals are very common. Grinding them up isn't necessary. Let them sit overnight or shake the solution hard for a while. When they're dissolved bring the solution to a gentle boil while constantly stirring so none of it burns. As soon as it starts boiling remove it from the heat and pour through 3 coffee filters layered together to filter out the unwanted filler crap.
Usually it is necessary to hold the filters like a bag with the liquid that didn't go through and gently squeeze to get the liquid to go through. Throw the mush left in the filter away. They dissolve easily to form a reddish or orange colored solution.
If CrO3 is being used, 21 ml is enough. These chemicals are thoroughly mixed together and allowed to sit for several hours with occasional stirring. After several hours LYE solution 1 part water, 1 part LYE is very slowly and carefully added dropwise with strong stirring until the solution is strongly basic pH 11 or more. This strong stirring is to make sure the cat is converted to the free base. Usually this is done with a sep funnel separatory funnel, which is a flask with a funnel-shaped bottom and a stopcock valve on the very bottom.
Sep funnels are used for separating liquids by opening the valve on the bottom and letting the bottom-most layer of liquid drain out. For safety, the bottle would need to be quot;burpedquot; often anyway to make sure no gasses build up in it. A large eyedropper-type tool could be used to efficiently remove the cat layer. Shake really hard, then allow it to separate. Insufficent shaking will result in poor yield with some undissolved cat base remaining in the spent sludge layer.
The water layer should be orange mixed with green. The green may settle out as a heavy sludge. Any remaining water-soluble impurities are dissolved into the water layer and not the TOLUENE layer and thus they're quot;washedquot; out. Here are 2 methods for doing this. A bottle is selected for holding the gas-producing mixture and a 1-hole stopper will be put in the top of the bottle. It should reach the bottom of the mixture. The surface of the paste should be rough with lots of holes poked into it for good gas production.
This gas goes out of the gas-producing bottle through the glass tube and bubbles through the TOLUENE-cat solution turning cat free base into cat salt. The cat salt should appear as crystals and after a while the solution should be thick with them. The crystals are recovered by pouring through a filter. Keep it up until the pH is low, staying well below 7 pH below 7 is acidic , then remove the solvent layer and keep for reuse. Check the pH, make sure it is 7 neutral or higher. This practical method avoids the mess of producing HCl gas.
HCl is a white gas that burns your eyes and nose really badly should you breathe it. It is sold in lab cylinders by chem supply houses and is not watched by the DEA. Just stick on a regulator, affix the rubber hose with a glass extension for submersion in the solvent, and open the valve to expel the gas through the solvent to produce PURE cat HCl. The methcathinone is then converted to the free base for separation from the rest of the unwanted crap mixed with it.
The free base dissolves in toluene and not in water whereas the unwanted crap dissolves in water and not in toluene. Since water and toluene separate into 2 layers the toluene layer containing the cat free base is saved and the water layer thrown out. The toluene could probably be evaporated leaving crystals of cat free base which could probably be smoked but I haven't heard of anyone smoking it nor have I heard of its effects on the human body. The cat free base is converted to cat salt using dilute hydrochloric acid or anhydrous HCL gas.
Cat salt is soluble in water and not in toluene, just the opposite of the free base. Using HCL gas the salt produced has no water layer to dissolve in so it crystalizes out. Using dilute HCL the salt leaves the toluene layer as before but has a water layer the water diluting the HCL to dissolve in. This water layer is saved and the water evaporated, leaving methcathinone-HCL.
One brand is called quot;Toluolquot; from Parks. LYE- Available at most hardware stores. Even Safeway has it. One brand is quot;Red Devil Lyequot; which is used to unclog grease clogs in drains. HCl, also called 6.How to make methcathinone at home
email: [email protected] - phone:(662) 673-7585 x 6918